2-Acetylbiphenylene

Base Information

• Chemical Name: 2-Acetylbiphenylene
• CAS No.: 779-26-0
• Molecular Formula: C₁₄H₁₀O
• Molecular Weight: 194.233
• DSSTox Substance ID: DTXSID50402196
• Wikidata: Q82205571
• Mol file: 779-26-0.mol

Synonyms:2-Acetylbiphenylene;779-26-0;1-biphenylen-2-ylethanone;1-(biphenylen-2-yl)ethanone;Ethanone,1-(2-biphenylenyl)-;SCHEMBL7741754;DTXSID50402196;MBOITOZRTPXJIS-UHFFFAOYSA-N;1-(biphenylen-2-yl)ethan-1-one;AKOS025394841;FT-0632949;(1S,3S)-{1-formyl-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentyl}-carbamic acid tert-butyl ester

Chemical Property of 2-Acetylbiphenylene

Chemical Property:

• Vapor Pressure: 9.54E-05mmHg at 25°C
• Melting Point: 137-139 °C(lit.)
• Refractive Index: 1.745
• Boiling Point: 338.9 °C at 760 mmHg
• Flash Point: 147.9 °C
• PSA: 17.07000
• Density: 1.218 g/cm³
• LogP: 3.53660
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 194.073164938
• Heavy Atom Count: 15
• Complexity: 271

Purity/Quality:

99% ^*data from raw suppliers

2-ACETYLBIPHENYLENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)C1=CC2=C(C=C1)C3=CC=CC=C32

Technology Process of 2-Acetylbiphenylene

There total 2 articles about 2-Acetylbiphenylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

bisbenzocyclobutene (259-79-0) + acetyl chloride (75-36-5) → 2-acetylbiphenylene (779-26-0)

Guidance literature:

With aluminium trichloride; In carbon disulfide; at 20 ℃; for 1.5h;

Reference yield:

→ 2-acetylbiphenylene (779-26-0)

Guidance literature:

Biphenylen, Acetylchlorid, AlCl3;

DOI:10.1021/ma60057a026

upstream raw materials:

bisbenzocyclobutene

acetyl chloride

Refernces