(Z)-3-(4-HYDROXY-PHENYL)-ACRYLIC ACID DOCOSYL ESTER

Base Information

• Chemical Name: (Z)-3-(4-HYDROXY-PHENYL)-ACRYLIC ACID DOCOSYL ESTER
• CAS No.: 145204-87-1
• Molecular Formula: C₃₁H₅₂O₃
• Molecular Weight: 472.752
• Mol file: 145204-87-1.mol

Synonyms:4'-hydroxy-cis-cinnamic acid docosyl ester

Chemical Property of (Z)-3-(4-HYDROXY-PHENYL)-ACRYLIC ACID DOCOSYL ESTER

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

(Z)-3-(4-HYDROXYPHENYL)ACRYLIC ACID DOCOSYLESTER 98.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-3-(4-HYDROXY-PHENYL)-ACRYLIC ACID DOCOSYL ESTER

There total 4 articles about (Z)-3-(4-HYDROXY-PHENYL)-ACRYLIC ACID DOCOSYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

C31H50O3 (1173709-64-2) → 4'-hydroxy-cis-cinnamic acid docosyl ester (145204-87-1)

Guidance literature:

With quinoline; 5% Pd-CaCO3; hydrogen; In ethyl acetate; at 20 ℃;

DOI:10.1248/cpb.57.476

Reference yield:

1-docosanol (661-19-8) → 4'-hydroxy-cis-cinnamic acid docosyl ester (145204-87-1)

Guidance literature:

Multi-step reaction with 2 steps

1: p-TsOH / acetone; benzene / 2 h / 80 °C

2: CHCl₃ / 0.5 h / Irradiation

With toluene-4-sulfonic acid; In chloroform; acetone; benzene;

DOI:10.1016/0031-9422(92)83497-M

Reference yield:

p-Coumaric Acid (7400-08-0,50940-26-6) → 4'-hydroxy-cis-cinnamic acid docosyl ester (145204-87-1)

Guidance literature:

Multi-step reaction with 2 steps

1: p-TsOH / acetone; benzene / 2 h / 80 °C

2: CHCl₃ / 0.5 h / Irradiation

With toluene-4-sulfonic acid; In chloroform; acetone; benzene;

DOI:10.1016/0031-9422(92)83497-M

upstream raw materials:

4'-hydroxy-trans-cinnamic acid docosyl ester

1-docosanol

p-Coumaric Acid

C₃₁H₅₀O₃

Refernces

• 1、 Hashidoko, Yasuyuki,Tahara, Satoshi,Mizutani, Junya. "LONG CHAIN ALKYL ESTERS OF 4'-HYDROXYCINNAMIC ACIDS FROM LEAVES OF ROSA RUGOSA". . p. 3282 - 3283. Retrieved 2007/10/02.