cycloocta[1,2-b:4,3-b':5,6-b:8,7-b']tetrathiophene

Base Information

• Chemical Name: cycloocta[1,2-b:4,3-b':5,6-b:8,7-b']tetrathiophene
• CAS No.: 51751-43-0
• Molecular Formula: C₁₆H₈S₄
• Molecular Weight: 328.504
• Mol file: 51751-43-0.mol

Synonyms:cycloocta[1,2-b:4,3-b':5,6-b:8,7-b']tetrathiophene

Chemical Property of cycloocta[1,2-b:4,3-b':5,6-b:8,7-b']tetrathiophene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cycloocta[1,2-b:4,3-b':5,6-b:8,7-b']tetrathiophene

There total 1 articles about cycloocta[1,2-b:4,3-b':5,6-b:8,7-b']tetrathiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-bithiophene (3172-56-3) → cycloocta[1,2-b:4,3-b':5,6-b:8,7-b']tetrathiophene (51751-43-0)

Guidance literature:

Multi-step reaction with 4 steps

1: N-Bromosuccinimide; acetic acid / chloroform

2: lithium diisopropyl amide

3: n-butyllithium; copper dichloride

4: trifluoroacetic acid / chloroform / 1 h / 20 °C

With N-Bromosuccinimide; n-butyllithium; acetic acid; trifluoroacetic acid; copper dichloride; lithium diisopropyl amide; In chloroform;

DOI:10.1039/d1cc03219d

upstream raw materials:

3,3'-bithiophene

Refernces