N-(NAPHTH-1-YL)MALEAMIC ACID

Base Information

• Chemical Name: N-(NAPHTH-1-YL)MALEAMIC ACID
• CAS No.: 119206-63-2
• Molecular Formula: C₁₄H₁₁NO₃
• Molecular Weight: 241.246
• Mol file: 119206-63-2.mol

Synonyms:2-Butenoicacid, 4-(1-naphthalenylamino)-4-oxo-, (E)- (9CI)

Chemical Property of N-(NAPHTH-1-YL)MALEAMIC ACID

Chemical Property:

• PSA: 66.40000
• LogP: 2.49210

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(NAPHTH-1-YL)MALEAMIC ACID

There total 2 articles about N-(NAPHTH-1-YL)MALEAMIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

maleic anhydride (108-31-6) + 1-amino-naphthalene (134-32-7) → N-(1-naphthyl)maleamic acid (119206-63-2,6973-77-9)

Guidance literature:

at 20 ℃;

DOI:10.3109/14756366.2015.1071808

Reference yield:

→ N-(1-naphthyl)maleamic acid (119206-63-2,6973-77-9)

Guidance literature:

Maleinsaeureanhydrid, α-Naphthylamin, k.Bzl.;

Reference yield: 70.0%

N-(1-naphthyl)maleamic acid (119206-63-2,6973-77-9) → N-(1-naphthalenyl)maleimide (3369-39-9)

Guidance literature:

With phosphorus pentaoxide; sulfuric acid; at 65 ℃; for 3h;

upstream raw materials:

maleic anhydride

1-amino-naphthalene

Downstream raw materials:

N-[1]naphthyl-maleamic acid methyl ester

N-(1-naphthalenyl)maleimide

N²-benzyl-N⁴-[1]naphthyl-asparagine

C₄₃H₂₇NO₃

Refernces

• 1、 Parvez, Masood,Ali, Saqib,Ahmad, Sajjad,Bhatti, Moazzam Hussain,Mazhar, Muhammad. "catena-poly[[tri-n-butyltin]-μ-N-(1-naphthyl)maleamato]". . p. m334-m335. Retrieved 2002.
• 2、 Jia, Qianfa,Chen, Lei,Yang, Gongming,Wang, Jian,Wei, Jia,Du, Zhiyun. "DABCO-catalyzed [3+2] cycloaddition reactions of azomethine imines with N-aryl maleimides: Facile access to dinitrogen-fused heterocycles". supporting information. p. 7150 - 7153. Retrieved 2015/12/12.
• 3、 Hiran,Chaudhary, Jyoti,Meena, Suresh,Paliwal, Shiv Narayan. "AIBN initiated free radical homopolymerization of N-(1-naphthyl)maleimide and copolymerization with MMA: Synthesis and characterization". experimental part. p. 607 - 614. Retrieved 2009/07/18.