Technology Process of 3-(p-methoxyphenyl)-2-phenylthiophene
There total 4 articles about 3-(p-methoxyphenyl)-2-phenylthiophene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide; hydrogen;
palladium on activated charcoal;
In
methanol;
at 40 ℃;
for 1.5h;
under 760 Torr;
DOI:10.1246/bcsj.67.2187
- Guidance literature:
-
Multi-step reaction with 4 steps
1: SO2Cl2 / CCl4 / 8 h / Heating
2: 66 percent / KI, KNO3, acetic acid / 0.5 h / Heating
3: 47 percent / bis(acetylacetonato)nickel(II), PPh3 / diethyl ether / 1 h / Ambient temperature
4: 83 percent / H2, KOH / 10percent Pd/C / methanol / 1.5 h / 40 °C / 760 Torr
With
bis(acetylacetonate)nickel(II); potassium hydroxide; sulfuryl dichloride; hydrogen; acetic acid; potassium nitrate; triphenylphosphine; potassium iodide;
palladium on activated charcoal;
In
methanol; tetrachloromethane; diethyl ether;
DOI:10.1246/bcsj.67.2187
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 47 percent / bis(acetylacetonato)nickel(II), PPh3 / diethyl ether / 1 h / Ambient temperature
2: 83 percent / H2, KOH / 10percent Pd/C / methanol / 1.5 h / 40 °C / 760 Torr
With
bis(acetylacetonate)nickel(II); potassium hydroxide; hydrogen; triphenylphosphine;
palladium on activated charcoal;
In
methanol; diethyl ether;
DOI:10.1246/bcsj.67.2187