2-(3-bromophenyl)-2-oxoacetaldehyde

Base Information

• Chemical Name: 2-(3-bromophenyl)-2-oxoacetaldehyde
• CAS No.: 701-37-1
• Molecular Formula: C₈H₅BrO₂
• Molecular Weight: 213.03
• Mol file: 701-37-1.mol

Synonyms:2-(3-bromophenyl)-2-oxoacetaldehyde

Chemical Property of 2-(3-bromophenyl)-2-oxoacetaldehyde

Chemical Property:

Purity/Quality:

2-(3-bromophenyl)-2-oxoacetaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(3-bromophenyl)-2-oxoacetaldehyde

There total 4 articles about 2-(3-bromophenyl)-2-oxoacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,3'-dibromoacetophenone (18523-22-3) → 2-(3-bromophenyl)-2-oxoacetaldehyde (701-37-1)

Guidance literature:

In water; dimethyl sulfoxide; at 50 ℃; for 2.5h;

Reference yield:

1-(3-Bromophenyl)ethanone (2142-63-4) → 2-(3-bromophenyl)-2-oxoacetaldehyde (701-37-1)

Guidance literature:

With selenium(IV) oxide; In 1,4-dioxane; water; for 4h; Heating;

Reference yield:

3-bromostyrene (2039-86-3,25584-47-8) → 2-(3-bromophenyl)-2-oxoacetaldehyde (701-37-1)

Guidance literature:

With iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 80 ℃; for 3.5h;

DOI:10.1039/c5ra05671c

upstream raw materials:

1-(3-Bromophenyl)ethanone

3-bromostyrene

2,3'-dibromoacetophenone

Downstream raw materials:

(3-bromophenyl)-(9H-β-carbolin-1-yl)-methanone

1-(3-bromobenzoyl)-9H-β-carboline-3-carboxylic acid

4-(3-bromophenyl)-6,8-dimethylpyrimido[4,5-c]pyridazine-5,7(6H,8H)-dione

C₈H₇BrN₂O

Refernces

• 1、 Lipp, Alexander,Badir, Shorouk O.,Dykstra, Ryan,Gutierrez, Osvaldo,Molander, Gary A.. "Catalyst-Free Decarbonylative Trifluoromethylthiolation Enabled by Electron Donor-Acceptor Complex Photoactivation". supporting information. p. 3507 - 3520. Retrieved 2021/06/11.
• 2、 -. "SMALL MOLECULE INHIBITORS OF NF-kB INDUCING KINASE". Page/Page column 324. . Retrieved 2020/12/11.