Technology Process of 2-bromo-5-methoxy-benzaldehyde oxime
There total 5 articles about 2-bromo-5-methoxy-benzaldehyde oxime which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; hydroxylamine hydrochloride;
In
ethanol;
at 23 ℃;
for 12h;
DOI:10.1021/ja043682p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 8.7 g / aq. LiOH / tetrahydrofuran / 8 h / 23 °C
2: 96 percent / DMSO; (COCl)2; Et3N / CH2Cl2 / -78 - 20 °C
3: 99 percent / HONH2*HCl; aq. NaOH / ethanol / 12 h / 23 °C
With
lithium hydroxide; sodium hydroxide; oxalyl dichloride; hydroxylamine hydrochloride; dimethyl sulfoxide; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/ja043682p
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 86 percent / N-bromosuccinimide; AIBN / benzene / 1 h / Heating
2: dimethylformamide / 8 h / 80 °C
3: 8.7 g / aq. LiOH / tetrahydrofuran / 8 h / 23 °C
4: 96 percent / DMSO; (COCl)2; Et3N / CH2Cl2 / -78 - 20 °C
5: 99 percent / HONH2*HCl; aq. NaOH / ethanol / 12 h / 23 °C
With
lithium hydroxide; sodium hydroxide; N-Bromosuccinimide; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); hydroxylamine hydrochloride; dimethyl sulfoxide; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ja043682p