C₅₄H₃₇NOSi

Base Information

• Chemical Name: C₅₄H₃₇NOSi
• CAS No.: 1414941-54-0
• Molecular Formula: C₅₄H₃₇NOSi
• Molecular Weight: 743.979
• Mol file: 1414941-54-0.mol

Synonyms:C₅₄H₃₇NOSi

Chemical Property of C₅₄H₃₇NOSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₄H₃₇NOSi

There total 3 articles about C₅₄H₃₇NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborane-2-yl)phenyl)-9-hydrogencarbazole (870119-58-7) + (3-bromophenyl)(3-(dibenzo[b,d]furan-4-yl)phenyl)diphenylsilane (1414960-14-7) → C54H37NOSi (1414941-54-0)

Guidance literature:

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; toluene; Inert atmosphere; Reflux;

Reference yield:

diphenylsilyl dichloride (80-10-4) → C54H37NOSi (1414941-54-0)

Guidance literature:

Multi-step reaction with 3 steps

1: n-butyllithium / hexane; diethyl ether / -78 °C

2: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / Inert atmosphere; Reflux

3: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; water / Inert atmosphere; Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; n-butyllithium; potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; hexane; water; toluene;

Reference yield:

1,3-dibromobenzene (108-36-1) → C54H37NOSi (1414941-54-0)

Guidance literature:

Multi-step reaction with 3 steps

1: n-butyllithium / hexane; diethyl ether / -78 °C

2: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / Inert atmosphere; Reflux

3: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; water / Inert atmosphere; Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; n-butyllithium; potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; hexane; water; toluene;

upstream raw materials:

diphenylsilyl dichloride

1,3-dibromobenzene

9-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborane-2-yl)phenyl)-9-hydrogencarbazole

(3-bromophenyl)(3-(dibenzo[b,d]furan-4-yl)phenyl)diphenylsilane

Refernces