Tetrabenzyl-TitaniuM-(IV)

Base Information Edit

Chemical Name:Tetrabenzyl-TitaniuM-(IV)
CAS No.:17520-19-3
Molecular Formula:C₂₈H₂₈Ti
Molecular Weight:412.41
Hs Code.:
Mol file:17520-19-3.mol

Synonyms:tetrabenzyl titanium

Suppliers and Price of Tetrabenzyl-TitaniuM-(IV)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of Tetrabenzyl-TitaniuM-(IV) Edit

Chemical Property:

Purity/Quality:: 98%Min ^*data from raw suppliers

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Technology Process of Tetrabenzyl-TitaniuM-(IV)

There total 7 articles about Tetrabenzyl-TitaniuM-(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 117984-39-1
tribenzyltitaniumcobalt tetracarbonyl

: 17520-19-3
tetrabenzyl titanium

Guidance literature:: With C₆H₅CH₂Li; In ⁽²⁾H₈-toluene; byproducts: Li{Co(CO)4}; addn. of PhCH2Li soln. (-40°C) to Ti complex soln. at -40°C, 30 min; detn. by 1H-NMR;

Reference yield: 33.0%

: 7550-45-0
titanium tetrachloride

: 100-44-7
benzyl chloride

: 17520-19-3
tetrabenzyl titanium

Guidance literature:: benzyl chloride; With magnesium; In diethyl ether;

titanium tetrachloride; In diethyl ether; at -15 - 20 ℃; for 0.5h;
DOI:10.1002/anie.202001111

Reference yield:

: 7550-45-0
titanium tetrachloride

: 6921-34-2
benzylmagnesium chloride

: 17520-19-3
tetrabenzyl titanium

Guidance literature:: In diethyl ether; pentane; to soln. C6H5CH2MgCl in Et2O at -15°C soln. TiCl4 in pentane was added dropwise over 2 h, react. mixt. was stirred at -15°C for 3 h; soln. was filtered, residue was washed with Et2O, combined filtrate and washings were evapd. in vacuo, dissolved in pentane, concd., and cooled to -30°C overnight;
DOI:10.1021/ja710288g