N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide

Base Information Edit

Chemical Name:N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide
CAS No.:152302-94-8
Molecular Formula:C₁₂H₁₇INO₄P
Molecular Weight:397.15
Hs Code.:
Mol file:152302-94-8.mol

Synonyms:N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide

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Chemical Property of N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide

There total 3 articles about N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3095-95-2
diethylphosphonoacetic acid

: 615-43-0
2-iodophenylamine

: 152302-94-8
N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide

Guidance literature:: With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1021/jo00077a018

Reference yield: 84.0%

: 1026051-79-5
triethyl phosphite

: 1339628-12-4
N-(2-iodophenyl)-2-bromoacetamide

: 152302-94-8
N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide

Guidance literature:: In 1,2-dichloro-ethane; at 90 ℃; for 4h;
DOI:10.1055/s-0036-1588956

Reference yield:

: 615-43-0
2-iodophenylamine

: 152302-94-8
N-(2-Iodophenyl)-α-(diethoxyphosphinyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 0 °C

2: 1,2-dichloro-ethane / 4 h / 90 °C

With triethylamine; In dichloromethane; 1,2-dichloro-ethane; 2: |Arbuzov Reaction;
DOI:10.1055/s-0036-1588956