5-isopropyl-1,3-dimethyl-4-nitrobenzene

Base Information

• Chemical Name: 5-isopropyl-1,3-dimethyl-4-nitrobenzene
• CAS No.: 132228-31-0
• Molecular Formula: C₁₁H₁₅NO₂
• Molecular Weight: 193.246
• Mol file: 132228-31-0.mol

Synonyms:5-isopropyl-1,3-dimethyl-4-nitrobenzene

Chemical Property of 5-isopropyl-1,3-dimethyl-4-nitrobenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 5-isopropyl-1,3-dimethyl-4-nitrobenzene

There total 2 articles about 5-isopropyl-1,3-dimethyl-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethylcumene (4706-90-5) → 5-isopropyl-1,3-dimethyl-4-nitrobenzene (132228-31-0)

Guidance literature:

With nitronium tetrafluoborate; In sulfolane;

DOI:10.1021/ja01060a020

Reference yield:

3,5-dimethylcumene (4706-90-5) → 5-isopropyl-1,3-dimethyl-2-nitrobenzene (132228-30-9) + 5-isopropyl-1,3-dimethyl-4-nitrobenzene (132228-31-0)

Guidance literature:

With nitric acid; acetic anhydride; acetic acid; for 2h; Overall yield = 71 %; Overall yield = 4.38 g;

DOI:10.1002/chem.201504404

Reference yield:

5-isopropyl-1,3-dimethyl-4-nitrobenzene (132228-31-0) → 2,4-dimethylnitrobenzene (89-87-2,156617-89-9,37551-97-6)

Guidance literature:

With trifluorormethanesulfonic acid; at 80 ℃;

DOI:10.1039/P29900001681

upstream raw materials:

3,5-dimethylcumene

Downstream raw materials:

2,4-dimethylnitrobenzene

Refernces