homoallyl phenylthiomethyl ether

Base Information

• Chemical Name: homoallyl phenylthiomethyl ether
• CAS No.: 212377-97-4
• Molecular Formula: C₁₁H₁₄OS
• Molecular Weight: 194.298
• Mol file: 212377-97-4.mol

Synonyms:homoallyl phenylthiomethyl ether

Chemical Property of homoallyl phenylthiomethyl ether

Chemical Property:

Purity/Quality:

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Technology Process of homoallyl phenylthiomethyl ether

There total 1 articles about homoallyl phenylthiomethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

phenylthiomethyl chloride (7205-91-6) + homoalylic alcohol (627-27-0) → homoallyl phenylthiomethyl ether (212377-97-4)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; sodium hydride; at 0 - 20 ℃; for 15.5h;

DOI:10.1021/jo980601x

Reference yield: 51.0%

1-Iodoheptane (4282-40-0) + homoallyl phenylthiomethyl ether (212377-97-4) → 1-(homoallyloxy)-1-(phenylthio)octane (195884-38-9)

Guidance literature:

homoallyl phenylthiomethyl ether; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -40 ℃; for 1h;

1-Iodoheptane; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1021/jo980601x

Reference yield:

homoallyl phenylthiomethyl ether (212377-97-4) → (1-But-3-enyloxy-decylsulfanyl)-benzene (119010-67-2)

Guidance literature:

With n-butyllithium;

DOI:10.1016/0040-4039(96)00516-3

upstream raw materials:

phenylthiomethyl chloride

homoalylic alcohol

Downstream raw materials:

(1-But-3-enyloxy-decylsulfanyl)-benzene

1-(homoallyloxy)-1-(phenylthio)octane

Refernces