C₁₄H₁₈O₃

Base Information Edit

Chemical Name:C₁₄H₁₈O₃
CAS No.:1312589-93-7
Molecular Formula:C₁₄H₁₈O₃
Molecular Weight:234.295
Hs Code.:
Mol file:1312589-93-7.mol

C<sub>14</sub>H<sub>18</sub>O<sub>3</sub>

Synonyms:C₁₄H₁₈O₃

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Chemical Property of C₁₄H₁₈O₃ Edit

Chemical Property:

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Technology Process of C₁₄H₁₈O₃

There total 8 articles about C₁₄H₁₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-p-tolyl-tetrahydro-pyran-2-ol

: 108-24-7
acetic anhydride

: 1312589-93-7
C₁₄H₁₈O₃

Guidance literature:: With triethylamine; dmap; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 108-24-7
acetic anhydride

: δ-(4-methylphenyl)-δ-valerolactone

: 1312589-93-7
C₁₄H₁₈O₃

Guidance literature:: δ-(4-methylphenyl)-δ-valerolactone; With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 2h;

acetic anhydride; With triethylamine; dmap; In dichloromethane; at 0 - 20 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 4294-57-9
para-methylphenylmagnesium bromide

: 1312589-93-7
C₁₄H₁₈O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(I) bromide; lithium bromide / tetrahydrofuran / 18 h / 0 °C / Inert atmosphere

2.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 1 h / 50 °C

2.2: pH 1

3.1: potassium hydroxide; sodium tetrahydroborate / water / 10 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 18 h / 20 °C

5.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

5.2: -78 - 20 °C

6.1: triethylamine / dmap / dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; lithium hydroxide monohydrate; water; diisobutylaluminium hydride; triethylamine; trifluoroacetic acid; potassium hydroxide; copper(I) bromide; lithium bromide; dmap; In tetrahydrofuran; dichloromethane; water;