1-N-Phenylcarbamoyl-1-cyanopyridinium ylid

Base Information

• Chemical Name: 1-N-Phenylcarbamoyl-1-cyanopyridinium ylid
• CAS No.: 129345-79-5
• Molecular Formula: C₁₄H₁₁N₃O
• Molecular Weight: 237.261
• Mol file: 129345-79-5.mol

Synonyms:1-N-Phenylcarbamoyl-1-cyanopyridinium ylid

Chemical Property of 1-N-Phenylcarbamoyl-1-cyanopyridinium ylid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-N-Phenylcarbamoyl-1-cyanopyridinium ylid

There total 1 articles about 1-N-Phenylcarbamoyl-1-cyanopyridinium ylid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

2-pyridin-1-ium-1-ylacetonitrile chloride (17281-59-3) + phenyl isocyanate (103-71-9) → 1-N-Phenylcarbamoyl-1-cyanopyridinium ylid (129345-79-5)

Guidance literature:

With triethylamine; In toluene; for 2h;

DOI:10.1007/BF00473865

Reference yield: 27.0%

1-N-Phenylcarbamoyl-1-cyanopyridinium ylid (129345-79-5) → 2-(2-N-Phenylcarbamoyl-1-amino-1-thio)ethylenepyridinium ylid (129345-78-4)

Guidance literature:

With hydrogen sulfide; triethylamine; In toluene; at 100 ℃; for 4h;

DOI:10.1007/BF00473865

upstream raw materials:

2-pyridin-1-ium-1-ylacetonitrile chloride

phenyl isocyanate

Downstream raw materials:

2-(2-N-Phenylcarbamoyl-1-amino-1-thio)ethylenepyridinium ylid

Refernces