C₂₅H₃₇SiNO₆

Base Information Edit

Chemical Name:C₂₅H₃₇SiNO₆
CAS No.:943542-54-9
Molecular Formula:C₂₅H₃₇NO₆Si
Molecular Weight:475.657
Hs Code.:
Mol file:943542-54-9.mol

C<sub>25</sub>H<sub>37</sub>SiNO<sub>6</sub>

Synonyms:C₂₅H₃₇SiNO₆

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Chemical Property of C₂₅H₃₇SiNO₆ Edit

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Technology Process of C₂₅H₃₇SiNO₆

There total 18 articles about C₂₅H₃₇SiNO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 943542-53-8
C₂₂H₂₉NO₆

: 75-77-4
chloro-trimethyl-silane

: 943542-54-9
C₂₅H₃₇SiNO₆

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ol0706051

Reference yield:

: 943542-50-5
C₁₅H₂₃NO₆

: 943542-54-9
C₂₅H₃₇SiNO₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: 8.8 g / t-BuOK / tetrahydrofuran / 6 h / 20 °C

2.1: lithium borohydride / tetrahydrofuran / 0.5 h / 20 °C

2.2: tetrahydrofuran; methanol / 24 h / 20 °C

3.1: 3.9 g / NMO; TPAP / CH₂Cl₂ / 18 h / 20 °C

4.1: tetrahydrofuran / 11.5 h / -78 - 20 °C

4.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C

5.1: aq. HCl / tetrahydrofuran / 10 h / 60 °C

6.1: NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

7.1: 136 mg / triethylamine / CH₂Cl₂ / 10 h / 20 °C

8.1: 94 percent / 1,3-propanedithiol; aq. HCl / 2,2,2-trifluoro-ethanol / 4 h / 60 °C

9.1: 53 percent / triethylamine / CH₂Cl₂ / 12 h / 20 °C

With 1.3-propanedithiol; hydrogenchloride; sodium tetrahydroborate; lithium borohydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; potassium tert-butylate; triethylamine; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; water;
DOI:10.1021/ol0706051

Reference yield:

: 1165952-91-9
cyclohexa-1,3-diene

: 943542-54-9
C₂₅H₃₇SiNO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran / 48 h / 20 °C

2.1: tetrahydrofuran / 11.5 h / -78 - 20 °C

2.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C

3.1: aq. HCl / tetrahydrofuran / 10 h / 60 °C

4.1: NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

5.1: 136 mg / triethylamine / CH₂Cl₂ / 10 h / 20 °C

6.1: 94 percent / 1,3-propanedithiol; aq. HCl / 2,2,2-trifluoro-ethanol / 4 h / 60 °C

7.1: 53 percent / triethylamine / CH₂Cl₂ / 12 h / 20 °C

With 1.3-propanedithiol; hydrogenchloride; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; water;
DOI:10.1021/ol0706051