N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride

Base Information

• Chemical Name: N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride
• CAS No.: 134433-51-5
• Molecular Formula: C₃₆H₅₃N₃*3ClH
• Molecular Weight: 637.22
• Mol file: 134433-51-5.mol

Synonyms:N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride

Chemical Property of N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride

There total 3 articles about N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

2-(4-Phenyl-butylcarbamoyl)-pentanedioic acid bis-[(4-phenyl-butyl)-amide] → N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride (134433-51-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1002/ardp.19913240411

Reference yield:

triethyl 1,1,3-propanetricarboxylate (2832-14-6) → N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride (134433-51-5)

Guidance literature:

Multi-step reaction with 2 steps

2: 55 percent / LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1002/ardp.19913240411

Reference yield:

4-phenyl-1-butylamine (13214-66-9) → N,N'-bis-(4-phenylbutyl)-2-(4-phenylbutylaminomethyl)-pentane-1,5-diamine trihydrochloride (134433-51-5)

Guidance literature:

Multi-step reaction with 2 steps

2: 55 percent / LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1002/ardp.19913240411

upstream raw materials:

triethyl 1,1,3-propanetricarboxylate

4-phenyl-1-butylamine

Refernces