3-Carbamoylpicolinic Acid

Base Information

• Chemical Name: 3-Carbamoylpicolinic Acid
• CAS No.: 4733-65-7
• Molecular Formula: C₇H₆N₂O₃
• Molecular Weight: 166.136
• Hs Code.: 2933399090
• European Community (EC) Number: 679-659-7
• DSSTox Substance ID: DTXSID80437976
• Nikkaji Number: J1.416.567C
• Wikidata: Q82253582
• Mol file: 4733-65-7.mol

Synonyms:3-carbamoyl-alpha-picolinic acid;3-carbamoyl-picolinic acid

Chemical Property of 3-Carbamoylpicolinic Acid

Chemical Property:

• Vapor Pressure: 1.54E-08mmHg at 25°C
• Refractive Index: 1.623
• Boiling Point: 440.6°Cat760mmHg
• Flash Point: 220.3°C
• PSA: 93.28000
• Density: 1.458g/cm³
• LogP: 0.57900
• XLogP3: 0.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 166.03784206
• Heavy Atom Count: 12
• Complexity: 205

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-Carbamoylpyridine-2-carboxylic Acid ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(N=C1)C(=O)O)C(=O)N

Technology Process of 3-Carbamoylpicolinic Acid

There total 2 articles about 3-Carbamoylpicolinic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-carbamoylpyridine-2-carboxylic acid (4733-65-7)

Guidance literature:

With ammonia; Behandeln mit Schwefeldioxyd;

Reference yield:

→ 3-carbamoylpyridine-2-carboxylic acid (4733-65-7)

Guidance literature:

Reference yield: 80.0%

methanol (67-56-1) + 3-carbamoylpyridine-2-carboxylic acid (4733-65-7) → methyl 3-cyanopyridine-2-carboxylate (53940-11-7)

Guidance literature:

With chloroformic acid ethyl ester; triethylamine;

Downstream raw materials:

methyl 3-cyanopyridine-2-carboxylate

3-cyanopyridine-2-carboxylic acid

3-cyanopyridine-2-carboxamide

Refernces