Technology Process of (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-(2,3-diethoxy-5-methylphenyl)-D-glucitol
There total 1 articles about (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-(2,3-diethoxy-5-methylphenyl)-D-glucitol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3,4-diethoxy-toluene; β-D-glucose pentaacetate;
With
silver trifluoroacetate; tin(IV) chloride;
In
dichloromethane; 1,2-dichloro-ethane;
at 0 - 20 ℃;
for 16h;
With
methanol; sodium methylate;
at 20 ℃;
acetic anhydride;
With
pyridine; dmap;
at 20 ℃;
for 48h;
- Guidance literature:
-
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile);
In
tetrachloromethane;
at 20 ℃;
for 0.5h;
Heating / reflux;