Technology Process of methyl 4-azido-2,3-di-O-benzyl-4,6-dideoxy-β-D-glucoside
There total 6 articles about methyl 4-azido-2,3-di-O-benzyl-4,6-dideoxy-β-D-glucoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide;
In
dimethyl sulfoxide;
for 0.0833333h;
DOI:10.1071/C96152
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 97 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
2: 1.8 g / dimethyl sulfoxide, oxalyl chloride / CH2Cl2 / 0.33 h / -65 °C
3: 80 percent / lithium tri-t-butoxyaluminohydride / diethyl ether / 0.33 h / 0 °C
4: 80 percent / pyridine / CH2Cl2 / -60 °C
5: 92 percent / sodium azide / dimethylsulfoxide / 0.08 h
With
pyridine; lithium aluminium tetrahydride; sodium azide; oxalyl dichloride; lithium tri(t-butoxy)aluminum hydride; dimethyl sulfoxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1071/C96152
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / lithium tri-t-butoxyaluminohydride / diethyl ether / 0.33 h / 0 °C
2: 80 percent / pyridine / CH2Cl2 / -60 °C
3: 92 percent / sodium azide / dimethylsulfoxide / 0.08 h
With
pyridine; sodium azide; lithium tri(t-butoxy)aluminum hydride;
In
diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1071/C96152
