Technology Process of C29H28ClFN4O6
There total 13 articles about C29H28ClFN4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
toluene;
at 70 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 11 steps
1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 100 °C
2: nitric acid; acetic acid / 0.33 h / -10 °C
3: iron; ammonium chloride / water; methanol / 105 °C
4: ammonium acetate; methanol / 100 °C
5: methanesulfonic acid; trifluoroacetic acid / 3 h / Reflux
6: pyridine / 3 h / 120 °C
7: thionyl chloride / N,N-dimethyl-formamide / 1.5 h / Reflux
8: methanol; ammonia / dichloromethane / 0.17 h / 80 °C
9: potassium carbonate / tetrahydrofuran / 20 °C
10: caesium carbonate / acetonitrile / 2 h / 50 °C
11: toluene / 3 h / 70 °C
With
pyridine; methanol; thionyl chloride; methanesulfonic acid; ammonium acetate; ammonia; nitric acid; iron; potassium carbonate; ammonium chloride; caesium carbonate; acetic acid; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 10 steps
1: nitric acid; acetic acid / 0.33 h / -10 °C
2: iron; ammonium chloride / water; methanol / 105 °C
3: ammonium acetate; methanol / 100 °C
4: methanesulfonic acid; trifluoroacetic acid / 3 h / Reflux
5: pyridine / 3 h / 120 °C
6: thionyl chloride / N,N-dimethyl-formamide / 1.5 h / Reflux
7: methanol; ammonia / dichloromethane / 0.17 h / 80 °C
8: potassium carbonate / tetrahydrofuran / 20 °C
9: caesium carbonate / acetonitrile / 2 h / 50 °C
10: toluene / 3 h / 70 °C
With
pyridine; methanol; thionyl chloride; methanesulfonic acid; ammonium acetate; ammonia; nitric acid; iron; potassium carbonate; ammonium chloride; caesium carbonate; acetic acid; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;