Technology Process of O-dibenzylisolariciresinol
There total 6 articles about O-dibenzylisolariciresinol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 1h;
Ambient temperature;
DOI:10.3987/R-1987-05-1169
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) lithium hexamethyldisilylamide (LHDS) / 1.) benzene, 2.) benzene, 0 deg C, 5 min
2: 78 percent / 60percent aq. perchloric acid / acetic acid; CH2Cl2 / 4.5 h / Ambient temperature
3: 80 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature
With
lithium aluminium tetrahydride; perchloric acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.3987/R-1987-05-1169
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) lithium hexamethyldisilylamide (LHDS) / 1.) benzene, 2.) benzene, 0 deg C, 5 min
2: 78 percent / 60percent aq. perchloric acid / acetic acid; CH2Cl2 / 4.5 h / Ambient temperature
3: 80 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature
With
lithium aluminium tetrahydride; perchloric acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.3987/R-1987-05-1169
