fluorodiphenylphosphine

Base Information

• Chemical Name: fluorodiphenylphosphine
• CAS No.: 20472-53-1
• Molecular Formula: C₁₂H₁₀FP
• Molecular Weight: 204.184
• Mol file: 20472-53-1.mol

Synonyms:fluorodiphenylphosphine

Chemical Property of fluorodiphenylphosphine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of fluorodiphenylphosphine

There total 3 articles about fluorodiphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.5%

chloro-diphenylphosphine (1079-66-9,74391-44-9) → fluorodiphenylphosphine (20472-53-1)

Guidance literature:

With sodium fluoride; In acetonitrile;

DOI:10.1021/jo00372a016

Reference yield:

1-(di-phenylphosphino)imidazole (54877-59-7) → 1-benzoylimidazole (10364-94-0) + fluorodiphenylphosphine (20472-53-1)

Guidance literature:

With benzoyl fluoride; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

→ fluorodiphenylphosphine (20472-53-1)

Guidance literature:

Aus Diphenylphosphinylchlorid u. NH4F;

upstream raw materials:

chloro-diphenylphosphine

1-(di-phenylphosphino)imidazole

Downstream raw materials:

diphenyltrifluorophosphorane

tetraphenyldiphosphine oxide

Tetraphenyldiphosphin

Refernces

• 1、 Dabkowski, Wojciech,Michalski, Jan,Wasiak, Jacek,Cramer, Friedrich. "New General Synthesis of Organophosphorus P-F Compounds via Reaction of Azolides of Phosphorus Acids with Acyl Fluorides: Novel Route to 2-Deoxynucleosidyl Phosphorofluoridates and Phosphorodifluoridates". . p. 817 - 820. Retrieved 2007/10/02.