phenyl 4-oxo-4-(1H-pyrrol-2-yl)butaneselenoate

Base Information

• Chemical Name: phenyl 4-oxo-4-(1H-pyrrol-2-yl)butaneselenoate
• CAS No.: 1052104-32-1
• Molecular Formula: C₁₄H₁₃NO₂Se
• Molecular Weight: 306.223
• Mol file: 1052104-32-1.mol

Synonyms:phenyl 4-oxo-4-(1H-pyrrol-2-yl)butaneselenoate

Chemical Property of phenyl 4-oxo-4-(1H-pyrrol-2-yl)butaneselenoate

Chemical Property:

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Technology Process of phenyl 4-oxo-4-(1H-pyrrol-2-yl)butaneselenoate

There total 1 articles about phenyl 4-oxo-4-(1H-pyrrol-2-yl)butaneselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-oxo-4-(1H-pyrrol-2-yl)butanoic acid (71739-65-6) + diphenyl diselenide (1666-13-3) → phenyl 4-oxo-4-(1H-pyrrol-2-yl)butaneselenoate (1052104-32-1)

Guidance literature:

With tributylphosphine; In dichloromethane; at -30 ℃; for 30h;

DOI:10.1016/j.tet.2008.06.014

Reference yield: 58.0%

phenyl 4-oxo-4-(1H-pyrrol-2-yl)butaneselenoate (1052104-32-1) → 2-propionylpyrrole (1073-26-3)

Guidance literature:

With azobis(2-cyanobutane); tri-n-butyl-tin hydride; In cyclohexane; acetonitrile; for 9h; Heating;

DOI:10.1016/j.tet.2008.06.014

upstream raw materials:

4-oxo-4-(1H-pyrrol-2-yl)butanoic acid

diphenyl diselenide

Downstream raw materials:

2-propionylpyrrole

Refernces