Technology Process of N--L-alanyl>-N-(indan-2-yl)glycine
There total 6 articles about N--L-alanyl>-N-(indan-2-yl)glycine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen bromide; acetic acid;
In
acetic acid;
for 0.166667h;
DOI:10.1248/cpb.34.2852
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 29 percent / H2, AcONa, AcOH, molecular sieves 3A / Raney Ni / ethanol
2: 93 percent / HCl / H2O / 4 h
3: 68 percent / diethyl phosphorocyanidate, Et3N / dimethylformamide / 1 h
4: 95 percent / HBr-AcOH 25percent / acetic acid / 0.17 h
With
hydrogenchloride; diethyl cyanophosphonate; 3 A molecular sieve; hydrogen bromide; hydrogen; sodium acetate; acetic acid; triethylamine;
nickel;
In
ethanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.2852
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 68 percent / diethyl phosphorocyanidate, Et3N / dimethylformamide / 1 h
2: 95 percent / HBr-AcOH 25percent / acetic acid / 0.17 h
With
diethyl cyanophosphonate; hydrogen bromide; acetic acid; triethylamine;
In
acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.2852
