BIS(2,2,2-TRIFLUOROETHYL)MALEATE

Base Information

• Chemical Name: BIS(2,2,2-TRIFLUOROETHYL)MALEATE
• CAS No.: 352-28-3
• Molecular Formula: C₈H₆F₆O₄
• Molecular Weight: 280.124
• Hs Code.: 2917190090
• Mol file: 352-28-3.mol

Synonyms:2-Butenedioicacid (2E)-, bis(2,2,2-trifluoroethyl) ester (9CI); 2-Butenedioic acid (E)-,bis(2,2,2-trifluoroethyl) ester; Fumaric acid, bis(2,2,2-trifluoroethyl) ester(6CI,8CI); Bis(1,1-dihydrotrifluoroethyl) fumarate

Chemical Property of BIS(2,2,2-TRIFLUOROETHYL)MALEATE

Chemical Property:

• Boiling Point: 225.1°Cat760mmHg
• Flash Point: 87.5°C
• PSA: 52.60000
• Density: 1.444g/cm³
• LogP: 1.75360

Purity/Quality:

98%min ^*data from raw suppliers

BIS-(2,2,2-TRIFLUOROETHYL) FUMARATE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BIS(2,2,2-TRIFLUOROETHYL)MALEATE

There total 1 articles about BIS(2,2,2-TRIFLUOROETHYL)MALEATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

fumaryl dichloride (627-63-4) + 2,2,2-trifluoroethanol (75-89-8) → bis(2,2,2-trifluoroethyl) fumarate (352-28-3)

Guidance literature:

Reference yield:

4,4'-diaminodicyclohexylmethane (1761-71-3) + bis(2,2,2-trifluoroethyl) fumarate (352-28-3) → C29H38F12N2O8

Guidance literature:

at 80 ℃; for 48h;

Reference yield:

3-aminomethyl-3,5,5-trimethylcyclohexylamine (2855-13-2) + bis(2,2,2-trifluoroethyl) fumarate (352-28-3) → C26H34F12N2O8

Guidance literature:

at 90 ℃; for 30h;

upstream raw materials:

fumaryl dichloride

2,2,2-trifluoroethanol

Refernces

• 1、 Hafez, Ahmed M.,Dudding, Travis,Wagerle, Ty. R.,Shah, Meha H.,Taggi, Andrew E.,Lectka, Thomas. "A multistage, one-pot procedure mediated by a single catalyst: A new approach to the catalytic asymmetric synthesis of β-amino acids". . p. 5819 - 5825. Retrieved 2007/10/03.