Technology Process of 5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione
There total 6 articles about 5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic anhydride;
In
acetic acid;
at 120 ℃;
for 1h;
DOI:10.1021/ma012113o
- Guidance literature:
-
C36H22N2O16;
With
pyridine; acetic anhydride; acetic acid;
at 115 ℃;
With
acetic anhydride; acetic acid;
at 120 ℃;
for 1h;
DOI:10.1021/ma021328a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / 48 h / 20 °C
2: potassium hydroxide / H2O / 4 h / 136 °C
3: potassium carbonate / N,N-dimethyl-acetamide
4: acetic anhydride / acetic acid / 1 h / 120 °C
With
potassium hydroxide; acetic anhydride; potassium carbonate;
In
N,N-dimethyl acetamide; water; acetic acid;
DOI:10.1021/ma012113o