Technology Process of C35H55NO6
There total 3 articles about C35H55NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; diisopropyl-carbodiimide;
In
N,N-dimethyl-formamide;
at 0 - 25 ℃;
for 72h;
Inert atmosphere;
DOI:10.1039/c0cc05635a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; benzenesulfonyl chloride / 48.4 h / -18 - 0 °C
2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 15.25 h / -20 - -18 °C
3: dmap; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 72 h / 0 - 25 °C / Inert atmosphere
With
pyridine; dmap; tetrabutyl ammonium fluoride; acetic acid; benzenesulfonyl chloride; diisopropyl-carbodiimide;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05635a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 15.25 h / -20 - -18 °C
2: dmap; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 72 h / 0 - 25 °C / Inert atmosphere
With
dmap; tetrabutyl ammonium fluoride; acetic acid; diisopropyl-carbodiimide;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05635a