2,4,6-tri(t-butyl)phenyl-2,6-di(isopropyl)phenyliminoborane

Base Information

• Chemical Name: 2,4,6-tri(t-butyl)phenyl-2,6-di(isopropyl)phenyliminoborane
• CAS No.: 152240-94-3
• Molecular Formula: C₃₀H₄₆BN
• Molecular Weight: 431.513
• Mol file: 152240-94-3.mol

Synonyms:2,4,6-tri(t-butyl)phenyl-2,6-di(isopropyl)phenyliminoborane

Chemical Property of 2,4,6-tri(t-butyl)phenyl-2,6-di(isopropyl)phenyliminoborane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2,4,6-tri(t-butyl)phenyl-2,6-di(isopropyl)phenyliminoborane

There total 1 articles about 2,4,6-tri(t-butyl)phenyl-2,6-di(isopropyl)phenyliminoborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2,4,6-tri-t-butylphenyldifluoroborane (129161-76-8) + lithium (2,6-diisopropylphenyl)amide → 2,4,6-tri(t-butyl)phenyl-2,6-di(isopropyl)phenyliminoborane (152240-94-3) + 2,6-diisopropylbenzenamine (24544-04-5)

Guidance literature:

In hexane; byproducts: LiF; dropping a soln. of 2,4,6-tri-t-butylphenyl-difluoroborane in n-hexane to a suspension of freshly lithiated 2,6-di(isopropyl)phenylamine in n-hexane cooled with ice (under N2) followed by refluxing for 3 h; removal of the solvent under reduced pressure and subliming the iminoborane from the residue in anoil pump vacuum, elem. anal.;

upstream raw materials:

2,4,6-tri-t-butylphenyldifluoroborane