C₁₇H₂₀ClNO₄

Base Information

• Chemical Name: C₁₇H₂₀ClNO₄
• CAS No.: 1258864-00-4
• Molecular Formula: C₁₇H₂₀ClNO₄
• Molecular Weight: 337.803
• Mol file: 1258864-00-4.mol

Synonyms:C₁₇H₂₀ClNO₄

Chemical Property of C₁₇H₂₀ClNO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₀ClNO₄

There total 3 articles about C₁₇H₂₀ClNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H17NO2 → C17H20ClNO4 (1258864-00-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dmap; triethylamine / dichloromethane / 0.5 h / 20 °C

1.2: 2 h / 20 °C

2.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / water; acetonitrile / 15 h / 0 °C

3.1: methanol / diethyl ether / 0 °C

With methanol; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; triethylamine; In diethyl ether; dichloromethane; water; acetonitrile;

DOI:10.3987/COM-10-12042

Reference yield:

C16H20ClNO3 (1258863-99-8) → C17H20ClNO4 (1258864-00-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / water; acetonitrile / 15 h / 0 °C

2: methanol / diethyl ether / 0 °C

With methanol; 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; In diethyl ether; water; acetonitrile;

DOI:10.3987/COM-10-12042

Reference yield:

4-chloro-benzoyl chloride (122-01-0) → C17H20ClNO4 (1258864-00-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dmap; triethylamine / dichloromethane / 0.5 h / 20 °C

1.2: 2 h / 20 °C

2.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / water; acetonitrile / 15 h / 0 °C

3.1: methanol / diethyl ether / 0 °C

With methanol; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; triethylamine; In diethyl ether; dichloromethane; water; acetonitrile;

DOI:10.3987/COM-10-12042

upstream raw materials:

C₁₆H₂₀ClNO₃

4-chloro-benzoyl chloride

Downstream raw materials:

C₁₇H₁₈ClNO₃

C₁₉H₂₀ClNO₄

C₂₀H₂₄ClNO₄

C₂₀H₂₂ClNO₄

Refernces