Technology Process of N-[5-Methoxy-2-(1-methylethoxy)phenyl]-3-nitro-2-pyridinamine
There total 3 articles about N-[5-Methoxy-2-(1-methylethoxy)phenyl]-3-nitro-2-pyridinamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium acetate; acetic acid;
Heating;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94 percent / H2 / 10percent Pd/C / methanol / 5 h / 26 °C / 760 Torr
2: 59 percent / NaOAc, gl. AcOH / Heating
With
hydrogen; sodium acetate; acetic acid;
palladium on activated charcoal;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 72 percent / conc. HNO3 (d=1.42), propionic acid, gl. AcOH / 0.42 h / 0 °C
2: 94 percent / H2 / 10percent Pd/C / methanol / 5 h / 26 °C / 760 Torr
3: 59 percent / NaOAc, gl. AcOH / Heating
With
hydrogen; nitric acid; sodium acetate; acetic acid; propionic acid;
palladium on activated charcoal;
In
methanol;