4-[(Z)-2-dodecylthioethenyl]anisole

Base Information

• Chemical Name: 4-[(Z)-2-dodecylthioethenyl]anisole
• CAS No.: 863775-00-2
• Molecular Formula: C₂₁H₃₄OS
• Molecular Weight: 334.566
• Mol file: 863775-00-2.mol

Synonyms:4-[(Z)-2-dodecylthioethenyl]anisole

Chemical Property of 4-[(Z)-2-dodecylthioethenyl]anisole

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-[(Z)-2-dodecylthioethenyl]anisole

There total 1 articles about 4-[(Z)-2-dodecylthioethenyl]anisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-methoxyphenylacetylen (768-60-5) + 1-dodecylthiol (112-55-0) → 4-[(Z)-2-dodecylthioethenyl]anisole (863775-00-2)

Guidance literature:

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; caesium carbonate; In dimethyl sulfoxide; at 85 ℃; for 4h;

DOI:10.1021/jo050931z

Reference yield: 90.0%

4-[(Z)-2-dodecylthioethenyl]anisole (863775-00-2) + methylmagnesium bromide (75-16-1) → anethole (104-46-1,25086-72-0,63589-56-0)

Guidance literature:

With bis(triphenylphosphine)nickel(II) chloride; In diethyl ether; for 12h; Heating;

DOI:10.1021/jo050931z

Reference yield: 85.0%

4-[(Z)-2-dodecylthioethenyl]anisole (863775-00-2) + phenylmagnesium bromide → p-methoxystilbene (1694-19-5)

Guidance literature:

With bis(triphenylphosphine)nickel(II) chloride; In diethyl ether; for 12h; Heating;

DOI:10.1021/jo050931z

upstream raw materials:

4-methoxyphenylacetylen

1-dodecylthiol

Downstream raw materials:

anethole

p-methoxystilbene

Refernces