Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester

Base Information

• Chemical Name: Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester
• CAS No.: 117133-84-3
• Molecular Formula: C₁₃H₁₈O₂S₂
• Molecular Weight: 270.417
• Mol file: 117133-84-3.mol

Synonyms:Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester

Chemical Property of Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester

There total 4 articles about Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

metgoxycarbonylsulfenyl chloride (26555-40-8) + 2,3,4,5-Tetramethylthioanisol (117133-83-2) → Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester (117133-84-3)

Guidance literature:

With aluminium trichloride; In dichloromethane; for 4h; Ambient temperature;

Reference yield:

1,2,3,4-Tetramethylbenzene (488-23-3) → Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester (117133-84-3)

Guidance literature:

Multi-step reaction with 4 steps

1: ClSO₃H

2: Zn, H(+)

3: OH(-)

4: 31 percent / AlCl₃ / CH₂Cl₂ / 4 h / Ambient temperature

With chlorosulfonic acid; aluminium trichloride; hydroxide; hydrogen cation; zinc; In dichloromethane;

Reference yield:

2,3,4,5-tetramethylbenzene-1-sulfonic acid (4681-79-2) → Thiokohlensaeure-O-methyl-S-(2-methylmercapto-3,4,5,6-tetramethylphenyl) ester (117133-84-3)

Guidance literature:

Multi-step reaction with 3 steps

1: Zn, H(+)

2: OH(-)

3: 31 percent / AlCl₃ / CH₂Cl₂ / 4 h / Ambient temperature

With aluminium trichloride; hydroxide; hydrogen cation; zinc; In dichloromethane;

upstream raw materials:

metgoxycarbonylsulfenyl chloride

2,3,4,5-Tetramethylthioanisol

1,2,3,4-Tetramethylbenzene

2,3,4,5-tetramethylbenzene-1-sulfonic acid

Downstream raw materials:

Tetramethyl-1,2-dimercaptobenzol

Refernces