phenyltriethoxytitanium

Base Information Edit

Chemical Name:phenyltriethoxytitanium
CAS No.:95576-66-2
Molecular Formula:C₁₂H₂₀O₃Ti
Molecular Weight:260.169
Hs Code.:
Mol file:95576-66-2.mol

Synonyms:phenyltriethoxytitanium

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Chemical Property of phenyltriethoxytitanium Edit

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Technology Process of phenyltriethoxytitanium

There total 2 articles about phenyltriethoxytitanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3712-48-9
tris(ethoxy)monochloro titanium

: 100-58-3
phenylmagnesium bromide

: 95576-66-2
phenyltriethoxytitanium

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.joc.5b01787

Reference yield:

: 3712-48-9
tris(ethoxy)monochloro titanium

: 591-51-5
phenyllithium

: 95576-66-2
phenyltriethoxytitanium

Guidance literature:: In diethyl ether; hexane; byproducts: LiCl; soln. of (OEt)3TiCl in hexane was cooled to 0°C, PhLi in ether was added dropwise and mixture was stirred for 1 h at 20°C; solvents removed in vac.;;
DOI:10.1007/BF00953348