C₃₉H₆₂O₇Si₂

Base Information

• Chemical Name: C₃₉H₆₂O₇Si₂
• CAS No.: 1315567-82-8
• Molecular Formula: C₃₉H₆₂O₇Si₂
• Molecular Weight: 699.088
• Mol file: 1315567-82-8.mol

Synonyms:C₃₉H₆₂O₇Si₂

Chemical Property of C₃₉H₆₂O₇Si₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₉H₆₂O₇Si₂

There total 6 articles about C₃₉H₆₂O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C36H56O7Si2 (1315567-67-9) + allyl bromide (106-95-6) → C39H62O7Si2 (1315567-82-8)

Guidance literature:

With iodine; magnesium; In diethyl ether; at 0 ℃;

DOI:10.1038/nchem.1074

Reference yield:

C24H28O7 → C39H62O7Si2 (1315567-82-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 122 °C / neat (no solvent)

1.2: 20 °C

2.1: 1,2-dichloro-benzene / 250 °C / Microwave irradiation

3.1: iodine; magnesium / diethyl ether / 0 °C

With iodine; magnesium; In diethyl ether; 1,2-dichloro-benzene; 1.1: Claisen rearrangement;

DOI:10.1038/nchem.1074

Reference yield:

C18H23BrO3 → C39H62O7Si2 (1315567-82-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: isopropyl alcohol / 80 °C

2.1: 122 °C / neat (no solvent)

2.2: 20 °C

3.1: 1,2-dichloro-benzene / 250 °C / Microwave irradiation

4.1: iodine; magnesium / diethyl ether / 0 °C

With iodine; magnesium; In diethyl ether; 1,2-dichloro-benzene; isopropyl alcohol; 2.1: Claisen rearrangement;

DOI:10.1038/nchem.1074

upstream raw materials:

C₃₆H₅₆O₇Si₂

allyl bromide

(+)-dimethyl-2,3-O-isopropylidene-D-tartrate

benzyl bromide

Downstream raw materials:

C₃₉H₄₄O₁₀

C₃₉H₄₂O₁₀

C₂₉H₃₄O₁₀

C₃₉H₆₁BrO₆Si₂

Refernces