Technology Process of 1,6-Anhydro-4-O-benzyl-2,3-dideoxy-2,3-epimino-β-D-talopyranose
There total 5 articles about 1,6-Anhydro-4-O-benzyl-2,3-dideoxy-2,3-epimino-β-D-talopyranose which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at -15 - 20 ℃;
DOI:10.1135/cccc20010799
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: NaH / tetrahydrofuran; dimethylformamide / -15 °C
1.2: 63 percent / tetrabutylammonium iodide / tetrahydrofuran; dimethylformamide / -15 - 20 °C
2.1: 75 percent / aq. NaN3; ammonium chloride / 2-methoxy-ethanol / 210 h / 110 - 120 °C
3.1: 85 percent / pyridine / 42 h / 20 °C
4.1: 62 percent / LiAlH4 / tetrahydrofuran / -15 - 20 °C
With
pyridine; lithium aluminium tetrahydride; sodium azide; ammonium chloride; sodium hydride;
In
tetrahydrofuran; 2-methoxy-ethanol; N,N-dimethyl-formamide;
DOI:10.1135/cccc20010799
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: NaH / tetrahydrofuran; dimethylformamide / -15 °C
1.2: 63 percent / tetrabutylammonium iodide / tetrahydrofuran; dimethylformamide / -15 - 20 °C
2.1: 75 percent / aq. NaN3; ammonium chloride / 2-methoxy-ethanol / 210 h / 110 - 120 °C
3.1: 85 percent / pyridine / 42 h / 20 °C
4.1: 62 percent / LiAlH4 / tetrahydrofuran / -15 - 20 °C
With
pyridine; lithium aluminium tetrahydride; sodium azide; ammonium chloride; sodium hydride;
In
tetrahydrofuran; 2-methoxy-ethanol; N,N-dimethyl-formamide;
DOI:10.1135/cccc20010799