2-FORMYLAMINOSORBIT

Base Information

• Chemical Name: 2-FORMYLAMINOSORBIT
• CAS No.: 89182-60-5
• Molecular Formula: C₇H₁₅NO₆
• Molecular Weight: 209.199
• Mol file: 89182-60-5.mol

Synonyms:2-FORMYLAMINOSORBIT;N-FORMYLAMINOSORBIT;1-DEOXY-1-FORMAMIDOHEXITOL

Chemical Property of 2-FORMYLAMINOSORBIT

Chemical Property:

• Vapor Pressure: 0.002Pa at 20℃
• PSA: 130.25000
• Density: 1.45[at 20℃]
• LogP: -2.80490
• Water Solubility.: 205g/L at 20℃

Purity/Quality:

99.9% ^*data from raw suppliers

N-Formyl-1-amino-1-deoxy-D-glucitol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-FORMYLAMINOSORBIT

There total 3 articles about 2-FORMYLAMINOSORBIT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-amino-1-deoxy-D-galactitol (42015-13-4) + Methyl formate (107-31-3) → N-formyl-1-amino-1-deoxy-D-galactitol (89182-60-5)

Guidance literature:

In methanol; at 60 ℃; for 6h;

DOI:10.1016/j.molcatb.2014.12.003

Reference yield:

D-Galactose (59-23-4) → N-formyl-1-amino-1-deoxy-D-galactitol (89182-60-5)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogen / methanol / 50 °C / 7500.75 - 9000.9 Torr / Autoclave

2: hydrogen; palladium 10% on activated carbon / methanol / 50 °C / 7500.75 - 9000.9 Torr / Autoclave

3: methanol / 6 h / 60 °C

With palladium 10% on activated carbon; hydrogen; In methanol;

DOI:10.1016/j.molcatb.2014.12.003

Reference yield:

N-benzyl-1-amino-1-deoxy-D-galactitol (74410-49-4) → N-formyl-1-amino-1-deoxy-D-galactitol (89182-60-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / methanol / 50 °C / 7500.75 - 9000.9 Torr / Autoclave

2: methanol / 6 h / 60 °C

With palladium 10% on activated carbon; hydrogen; In methanol;

DOI:10.1016/j.molcatb.2014.12.003

upstream raw materials:

D-Galactose

N-benzyl-1-amino-1-deoxy-D-galactitol

1-amino-1-deoxy-D-galactitol

Methyl formate

Downstream raw materials:

N-formyl-1-amino-1-deoxy-5-keto-D-glucitol

Refernces