trimethylgermane

Base Information

• Chemical Name: trimethylgermane
• CAS No.: 92063-61-1
• Molecular Formula: C₃H₁₀Ge
• Molecular Weight: 119.694
• Mol file: 92063-61-1.mol

Synonyms:trimethylgermane

Chemical Property of trimethylgermane

Chemical Property:

Purity/Quality:

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Technology Process of trimethylgermane

There total 1 articles about trimethylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

d(4)-methanol (811-98-3) + trimethyltin(IV)chloride (1066-45-1) + (methyl)3GeSn(methyl)3 (16393-89-8) → chlorotrimethylgermane (1529-47-1) + tetramethylstannane (594-27-4) + trimethylgermane (92063-61-1)

Guidance literature:

In d⁽⁴⁾-methanol; a mixt. of Me3GeSnMe3 and Me3SnCl in CD3OD was kept for 30 h, reaction was followed by (1)H NMR spectroscopy; not isolated, identified by (1)H NMR spectrum;

DOI:10.1016/0022-328X(85)80065-6

Reference yield:

trimethylgermane (92063-61-1) → germanium (7440-56-4) + hexamethyldigermane (993-52-2)

Guidance literature:

In gas; byproducts: CH4, CH3D; react. at 673-873 K; IR monitoring; Kinetics;

DOI:10.1039/c39920000291

Reference yield:

trimethylgermane (92063-61-1) → hexamethyldigermoxane (2237-93-6)

Guidance literature:

With oxygen; In gas; byproducts: D2O; gas-phase autoxidn. of Ge-compd. at 493 K; monitored by IR; Kinetics;

DOI:10.1021/om00017a012

upstream raw materials:

d⁽⁴⁾-methanol

trimethyltin(IV)chloride

(methyl)3GeSn(methyl)3

Downstream raw materials:

germanium

hexamethyldigermane

hexamethyldigermoxane

Refernces