Technology Process of N-benzoyl-3'-triisopropylsilyl-5'-keto-8,5'-cyclo-2'-deoxyadenosine
There total 5 articles about N-benzoyl-3'-triisopropylsilyl-5'-keto-8,5'-cyclo-2'-deoxyadenosine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridine / 0 - 20 °C / Inert atmosphere
2.1: pyridine; 1H-imidazole; silver nitrate / 48 h / 0 - 20 °C / Inert atmosphere
3.1: sodium iodide / acetone / 4 h / Inert atmosphere; Reflux
4.1: pyridine; zinc / 4 h / 80 °C / Inert atmosphere
4.2: 2 h / Inert atmosphere; Reflux
5.1: selenium(IV) oxide / 1,4-dioxane / 1 h / Inert atmosphere; Reflux
With
pyridine; 1H-imidazole; selenium(IV) oxide; silver nitrate; sodium iodide; zinc;
In
1,4-dioxane; acetone;
DOI:10.1080/15257770.2012.716189
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine; 1H-imidazole; silver nitrate / 48 h / 0 - 20 °C / Inert atmosphere
2.1: sodium iodide / acetone / 4 h / Inert atmosphere; Reflux
3.1: pyridine; zinc / 4 h / 80 °C / Inert atmosphere
3.2: 2 h / Inert atmosphere; Reflux
4.1: selenium(IV) oxide / 1,4-dioxane / 1 h / Inert atmosphere; Reflux
With
pyridine; 1H-imidazole; selenium(IV) oxide; silver nitrate; sodium iodide; zinc;
In
1,4-dioxane; acetone;
DOI:10.1080/15257770.2012.716189