Technology Process of C15H18ClNO7*C7H9N*ClHO4
There total 7 articles about C15H18ClNO7*C7H9N*ClHO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: water
2: aq. ammonia / 24 h / 150 °C / bomb
3: 30percent H2O2, fuming H2SO4 / 1.) 10 deg C, several hours, 2.) room temperature, 2 d
4: 61 percent / SOCl2, dimethylformamide
5: benzene / 48 h / 50 °C
6: CD2Cl2 / reactions with other alkylammonium salts, ΔG(activation), exchange rate constants
With
ammonium hydroxide; thionyl chloride; sulfuric acid; water; dihydrogen peroxide; N,N-dimethyl-formamide;
In
dichloromethane-d2; benzene;
DOI:10.1021/ja00522a004
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. ammonia / 24 h / 150 °C / bomb
2: 30percent H2O2, fuming H2SO4 / 1.) 10 deg C, several hours, 2.) room temperature, 2 d
3: 61 percent / SOCl2, dimethylformamide
4: benzene / 48 h / 50 °C
5: CD2Cl2 / reactions with other alkylammonium salts, ΔG(activation), exchange rate constants
With
ammonium hydroxide; thionyl chloride; sulfuric acid; dihydrogen peroxide; N,N-dimethyl-formamide;
In
dichloromethane-d2; benzene;
DOI:10.1021/ja00522a004
- Guidance literature:
-
Multi-step reaction with 7 steps
1: PCl5 / CHCl3 / 72 h / Heating
2: water
3: aq. ammonia / 24 h / 150 °C / bomb
4: 30percent H2O2, fuming H2SO4 / 1.) 10 deg C, several hours, 2.) room temperature, 2 d
5: 61 percent / SOCl2, dimethylformamide
6: benzene / 48 h / 50 °C
7: CD2Cl2 / reactions with other alkylammonium salts, ΔG(activation), exchange rate constants
With
ammonium hydroxide; thionyl chloride; phosphorus pentachloride; sulfuric acid; water; dihydrogen peroxide; N,N-dimethyl-formamide;
In
chloroform; dichloromethane-d2; benzene;
DOI:10.1021/ja00522a004