Technology Process of 2-benzyl-7-methoxy-1-benzosuberene
There total 9 articles about 2-benzyl-7-methoxy-1-benzosuberene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
benzene;
for 0.5h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77 percent / KOH / methanol / 1.) 10 deg C, 30 min, 2.) room temperature, 4 h
2: 100 percent / hydrogen / 10 percent Pd-C / ethyl acetate / 760 Torr / Ambient temperature
3: 99 percent / KBH4 / methanol / 4 h / Ambient temperature
4: 100 percent / p-TsOH / benzene / 0.5 h / Heating
With
potassium hydroxide; potassium borohydride; hydrogen; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
methanol; ethyl acetate; benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: PCl5 / benzene / 0.5 h / Heating
2: SnCl4 / benzene / 24 h / Ambient temperature
3: 77 percent / KOH / methanol / 1.) 10 deg C, 30 min, 2.) room temperature, 4 h
4: 100 percent / hydrogen / 10 percent Pd-C / ethyl acetate / 760 Torr / Ambient temperature
5: 99 percent / KBH4 / methanol / 4 h / Ambient temperature
6: 100 percent / p-TsOH / benzene / 0.5 h / Heating
With
potassium hydroxide; potassium borohydride; phosphorus pentachloride; hydrogen; tin(IV) chloride; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
methanol; ethyl acetate; benzene;
