3-<2-1(-methoxyethyl)phenyl>propenoic acid 13C labelled in C2

Base Information

• Chemical Name: 3-<2-1(-methoxyethyl)phenyl>propenoic acid 13C labelled in C2
• CAS No.: 122244-58-0
• Molecular Formula: C₁₂H₁₄O₃
• Molecular Weight: 207.23
• Mol file: 122244-58-0.mol

Synonyms:3-<2-1(-methoxyethyl)phenyl>propenoic acid 13C labelled in C2

Chemical Property of 3-<2-1(-methoxyethyl)phenyl>propenoic acid 13C labelled in C2

Chemical Property:

Purity/Quality:

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Technology Process of 3-<2-1(-methoxyethyl)phenyl>propenoic acid 13C labelled in C2

There total 1 articles about 3-<2-1(-methoxyethyl)phenyl>propenoic acid 13C labelled in C2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[2-13C] malonic acid (55514-11-9) + 2-(1-methoxyethyl)benzaldehyde (135679-46-8) → 3-<2-1(-methoxyethyl)phenyl>propenoic acid 13C labelled in C2 (122244-58-0)

Guidance literature:

With piperidine; In pyridine; at 110 ℃; for 3h;

DOI:10.1016/0040-4020(89)80080-8

Reference yield: 82.0%

methanol (67-56-1) + 3-<2-1(-methoxyethyl)phenyl>propenoic acid 13C labelled in C2 (122244-58-0) → methyl 3<2-(1-methoxyethyl)phenyl>propenoate 13C labelled in C2 (122244-60-4)

Guidance literature:

With sulfuric acid; for 12h; Heating;

DOI:10.1016/0040-4020(89)80080-8

upstream raw materials:

[2-13C] malonic acid

2-(1-methoxyethyl)benzaldehyde

Downstream raw materials:

methyl 3<2-(1-methoxyethyl)phenyl>propenoate 13C labelled in C2

Refernces