N-benzylnicotiniminoyl chloride

Base Information

• Chemical Name: N-benzylnicotiniminoyl chloride
• CAS No.: 1611477-32-7
• Molecular Formula: C₁₃H₁₁ClN₂
• Molecular Weight: 230.697
• Mol file: 1611477-32-7.mol

Synonyms:N-benzylnicotiniminoyl chloride

Chemical Property of N-benzylnicotiniminoyl chloride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N-benzylnicotiniminoyl chloride

There total 2 articles about N-benzylnicotiniminoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzylnicotinamide (2503-55-1) → N-benzylnicotiniminoyl chloride (1611477-32-7)

Guidance literature:

With phosphorus pentachloride; In dichloromethane; at 20 ℃; for 1h; Schlenk technique;

DOI:10.1039/c4dt00372a

Reference yield:

3-pyridinecarbonyl chloride (10400-19-8) + benzylamine (100-46-9) → N-benzylnicotiniminoyl chloride (1611477-32-7)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C

2: phosphorus pentachloride / dichloromethane / 1 h / 20 °C

With phosphorus pentachloride; triethylamine; In dichloromethane;

upstream raw materials:

N-benzylnicotinamide

3-pyridinecarbonyl chloride

benzylamine

Refernces

• 1、 -. "METHOD FOR THE CATALYTIC REDUCTION OF ACID CHLORIDES AND IMIDOYL CHLORIDES". Paragraph 0141; 0142. . Retrieved 2014/08/19.