S-Cyanomethyl-S-dodecyltrithiocarbonate, min. 97%

Base Information

• Chemical Name: S-Cyanomethyl-S-dodecyltrithiocarbonate, min. 97%
• CAS No.: 796045-97-1
• Molecular Formula: C₁₅H₂₇NS₃
• Molecular Weight: 317.584
• Mol file: 796045-97-1.mol

Synonyms:Cyanomethyldodecyl trithiocarbonate

Chemical Property of S-Cyanomethyl-S-dodecyltrithiocarbonate, min. 97%

Chemical Property:

• Melting Point: 30-33°C
• Boiling Point: 462.2±24.0 °C(Predicted)
• Flash Point: >110℃
• PSA: 106.48000
• Density: 1.050±0.06 g/cm3(Predicted)
• LogP: 6.18218
• Storage Temp.: 2-8°C
• Sensitive.: light sensitive, store cold

Purity/Quality:

98%,99%, ^*data from raw suppliers

Cyanomethyl Dodecyl Trithiocarbonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-36/37/38
• Safety Statements: 36/39

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Reversible Addition Fragmentation Chain Transfer (RAFT) Polymerization

Technology Process of S-Cyanomethyl-S-dodecyltrithiocarbonate, min. 97%

There total 2 articles about S-Cyanomethyl-S-dodecyltrithiocarbonate, min. 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

carbon disulfide (75-15-0,12122-00-8) + chloroacetonitrile (107-14-2) + 1-dodecylthiol (112-55-0) → S-dodecyl-S'-cyanomethyl trithiocarbonate (796045-97-1)

Guidance literature:

1-dodecylthiol; With sodium hydroxide; In water; isopropyl alcohol; at 5 ℃; for 0.5h;

carbon disulfide; In water; isopropyl alcohol; at 0 - 5 ℃; for 0.666667h;

chloroacetonitrile; In water; isopropyl alcohol; at 0 - 5 ℃; for 2.33333h;

Reference yield:

chloroacetonitrile (107-14-2) + 1-dodecylthiol (112-55-0) → S-dodecyl-S'-cyanomethyl trithiocarbonate (796045-97-1) + 4-vinylphenyl glycidyl ether (2653-39-6)

Guidance literature:

With carbon disulfide; sodium hydroxide; In water; isopropyl alcohol; Petroleum ether;

upstream raw materials:

chloroacetonitrile

1-dodecylthiol

carbon disulfide

Refernces

• 1、 -. "Synthesis of trithiocarbonates". Page/Page column 1-2. . Retrieved 2010/11/27.