Technology Process of 2-methoxy-4-deuterioaniline
There total 5 articles about 2-methoxy-4-deuterioaniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
platinum(IV) oxide;
In
benzene;
Yield given;
DOI:10.1021/ja00335a035
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) boron trifluoride etherate, tert-butyl nitrite / 1.) CH2Cl2
2: hydrogen / platinum oxide / benzene
With
tert.-butylnitrite; boron trifluoride diethyl etherate; hydrogen;
platinum(IV) oxide;
In
benzene;
DOI:10.1021/ja00335a035
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride
3: 13 g / 85 °C / Hofmann rearrangement
4: 1.) boron trifluoride etherate, tert-butyl nitrite / 1.) CH2Cl2
5: hydrogen / platinum oxide / benzene
With
thionyl chloride; tert.-butylnitrite; boron trifluoride diethyl etherate; hydrogen;
platinum(IV) oxide;
In
benzene;
DOI:10.1021/ja00335a035
