Technology Process of C55H38N2S
There total 7 articles about C55H38N2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tri-tert-butyl phosphine; sodium t-butanolate;
palladium diacetate;
In
toluene;
at 100 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogensulfite / water / 12 h / 120 °C
2: potassium carbonate; copper; 18-crown-6 ether / 12 h / 180 °C
3: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 12 h / 100 °C
4: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 12 h / 100 °C
With
18-crown-6 ether; tri-tert-butyl phosphine; copper; potassium carbonate; sodium hydrogensulfite; sodium t-butanolate;
palladium diacetate;
In
water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogensulfite / water / 12 h / 120 °C
2: potassium carbonate; copper; 18-crown-6 ether / 12 h / 180 °C
3: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 12 h / 100 °C
4: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 12 h / 100 °C
With
18-crown-6 ether; tri-tert-butyl phosphine; copper; potassium carbonate; sodium hydrogensulfite; sodium t-butanolate;
palladium diacetate;
In
water; toluene;