Technology Process of C30H38N3O6P
There total 1 articles about C30H38N3O6P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium diisopropyl amide;
In
tetrahydrofuran; hexane;
at -60 - 20 ℃;
for 5h;
further reagent DBU, DMAP;
DOI:10.1246/bcsj.71.1887
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) hydrogen, 2.) NaHCO3 / 1.) 10percent Pd-C / 1.) methanol, 2 h, 2.) water, acetone, 0 deg C, 1 h , room temperature, 5 h
2: DCC / ethyl acetate / 3 h / 0 °C
3: DIEA, HOBt-H2O / CH2Cl2 / 7 h / 0 - 20 °C
4: aq. TFA / 12 h
With
hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
palladium on activated charcoal;
In
dichloromethane; ethyl acetate;
DOI:10.1246/bcsj.71.1887
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) hydrogen, 2.) NaHCO3 / 1.) 10percent Pd-C / 1.) methanol, 2 h, 2.) water, acetone, 0 deg C, 1 h , room temperature, 5 h
2: DCC / ethyl acetate / 3 h / 0 °C
3: DIEA, HOBt-H2O / CH2Cl2 / 7 h / 0 - 20 °C
With
hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
dichloromethane; ethyl acetate;
DOI:10.1246/bcsj.71.1887