cholest-5⁽⁶⁾en-3,7-diol

Base Information

• Chemical Name: cholest-5⁽⁶⁾en-3,7-diol
• CAS No.: 691013-43-1
• Molecular Formula: C₂₇H₄₆O₂
• Molecular Weight: 402.661
• Mol file: 691013-43-1.mol

Synonyms:cholest-5⁽⁶⁾en-3,7-diol

Chemical Property of cholest-5⁽⁶⁾en-3,7-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cholest-5⁽⁶⁾en-3,7-diol

There total 1 articles about cholest-5⁽⁶⁾en-3,7-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

7-ketocholesteryl acetate (809-51-8) → cholest-5(6)en-3,7-diol (691013-43-1) + cholest-5-ene-3β,7-diol 3-monoacetate (17974-77-5,19317-90-9,98674-04-5,77059-25-7)

Guidance literature:

With sodium tetrahydroborate; In 1,4-dioxane; methanol; at 0 - 20 ℃; for 3h; pH=8;

DOI:10.1016/j.steroids.2015.12.020

Reference yield: 47.0%

cholest-5(6)en-3,7-diol (691013-43-1) + tert-butyl alcohol (75-65-0) → cholest-3,5-dien-7-one (567-72-6) + cholest-5(6)epoxy-3,7-diol + A-nor-3-hydroxy-3-t-butoxy-cholest-5(6)en-7-one

Guidance literature:

With dihydrogen peroxide; toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 72h;

DOI:10.1016/j.steroids.2015.12.020

upstream raw materials:

7-ketocholesteryl acetate

Downstream raw materials:

cholest-3,5-dien-7-one

Refernces