Technology Process of C33H44N4O8
There total 11 articles about C33H44N4O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-bromo-1-(4-hydroxy-3-methoxy-5-nitrophenyl)ethanone; 3-(azacyclotridecan-1-yl)propan-1-amine;
With
sodium iodide;
In
dimethyl sulfoxide;
for 0.25h;
Inert atmosphere;
2-(4-hydroxy-3-methoxy-5-nitrophenyl)acetaldehyde;
In
methanol;
for 16h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere
3.1: sodium iodide / dimethyl sulfoxide / 0.25 h / Inert atmosphere
3.2: 16 h
With
lithium aluminium tetrahydride; triethylamine; sodium iodide;
In
diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / Inert atmosphere; Reflux
2.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere
4.1: sodium iodide / dimethyl sulfoxide / 0.25 h / Inert atmosphere
4.2: 16 h
With
lithium aluminium tetrahydride; triethylamine; sodium iodide;
In
tetrahydrofuran; diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;