triphenylantimony bis(pentafluorobenzoate)

Base Information

• Chemical Name: triphenylantimony bis(pentafluorobenzoate)
• CAS No.: 360572-79-8
• Molecular Formula: C₃₂H₁₅F₁₀O₄Sb
• Molecular Weight: 775.203
• Mol file: 360572-79-8.mol

Synonyms:triphenylantimony bis(pentafluorobenzoate)

Chemical Property of triphenylantimony bis(pentafluorobenzoate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of triphenylantimony bis(pentafluorobenzoate)

There total 1 articles about triphenylantimony bis(pentafluorobenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Pentafluorobenzoic acid (602-94-8) + triphenylantimony (603-36-1) → triphenylantimony bis(pentafluorobenzoate) (360572-79-8)

Guidance literature:

With dihydrogen peroxide; In diethyl ether; water; byproducts: H2O; addn. of acid and aq. H2O2 to a soln. of antimony compd. in ether, keeping for 12 h at 20°C; filtration, drying; elem. anal.;

DOI:10.1023/A:1015439500222

Reference yield: 86.0%

pentaphenylantimony (2170-05-0) + triphenylantimony bis(pentafluorobenzoate) (360572-79-8) → tetraphenylantimony pentafluorobenzoate (360572-77-6)

Guidance literature:

In toluene; heating a mixt. of antimony compds. in toluene at 90°C for 1 h; evapn., crystn. (toluene/heptane 1:1); elem. anal.;

DOI:10.1023/A:1015439500222

Reference yield: 69.0%

pentaphenylantimony (2170-05-0) + triphenylantimony bis(pentafluorobenzoate) (360572-79-8) → tetraphenylantimony pentafluorobenzoate

Guidance literature:

In toluene; 90°C, 1 h; solvent removed; residue recrystd. from toluene/heptane (1/1); elem. anal.;

DOI:10.1023/A:1015517216693

upstream raw materials:

Pentafluorobenzoic acid

triphenylantimony

Downstream raw materials:

tetraphenylantimony pentafluorobenzoate

Refernces

• 1、 Sharutin,Sharutina,Bondar',Pakusina,Adonin,Starichenko. "Synthesis of tetra- and triarylantimony fluorobenzoates". . p. 390 - 391. Retrieved 2007/10/03.