C₃₄H₃₂N₂O₄

Base Information

• Chemical Name: C₃₄H₃₂N₂O₄
• CAS No.: 1415036-61-1
• Molecular Formula: C₃₄H₃₂N₂O₄
• Molecular Weight: 532.639
• Mol file: 1415036-61-1.mol

Synonyms:C₃₄H₃₂N₂O₄

Chemical Property of C₃₄H₃₂N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₂N₂O₄

There total 3 articles about C₃₄H₃₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

3-hydroxybenzophenone (13020-57-0) + 4-(4-bromobutoxy)-N-(2-(1H-indol-3-yl)ethyl)benzamide (1415036-73-5) → C34H32N2O4 (1415036-61-1)

Guidance literature:

With potassium carbonate; In acetone; for 24h; Reflux;

DOI:10.1016/j.bmc.2012.09.016

Reference yield:

4-hydroxy-benzoic acid (99-96-7) → C34H32N2O4 (1415036-61-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide / tetrahydrofuran / 1 h / 0 °C

1.2: 24 h / 20 °C

2.1: potassium iodide; potassium carbonate / acetone; Petroleum ether / 72 h / 65 °C

3.1: potassium carbonate / acetone / 24 h / Reflux

With potassium carbonate; dicyclohexyl-carbodiimide; potassium iodide; In tetrahydrofuran; acetone; Petroleum ether;

DOI:10.1016/j.bmc.2012.09.016

Reference yield:

tryptamine (61-54-1) → C34H32N2O4 (1415036-61-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide / tetrahydrofuran / 1 h / 0 °C

1.2: 24 h / 20 °C

2.1: potassium iodide; potassium carbonate / acetone; Petroleum ether / 72 h / 65 °C

3.1: potassium carbonate / acetone / 24 h / Reflux

With potassium carbonate; dicyclohexyl-carbodiimide; potassium iodide; In tetrahydrofuran; acetone; Petroleum ether;

DOI:10.1016/j.bmc.2012.09.016

upstream raw materials:

3-hydroxybenzophenone

4-(4-bromobutoxy)-N-(2-(1H-indol-3-yl)ethyl)benzamide

tryptamine

4-hydroxy-benzoic acid

Refernces